Thionyl chloride (or thionyl dichloride) is an inorganic compound with the formula SOCl 2.SOCl 2 is a reactive chemical reagent used in chlorination reactions. 136.14 g/mol--1 1 1-11 3 °C--1.357 g. DMF. We doesn't provide density of thionyl chloride products or service, please contact them directly and verify their companies info carefully. . CAMEO Chemicals. Procedure excerpt: A mixture of the SM (1.0 g, 6.3 mmol) in ACN (20 mL) was treated with SOCl2 (0.8 mL). Gascheck Tesla helium leak detector . decomposes Solubility: reacts in HBr, acetone, and alcohol soluble in benzene, toluene, ether Structure Molecular shape. It is an aliphatic nitrile and a volatile organic compound. Acute toxicity Category 3; Skin corrosion/irritation Category 1 A; Serious eye damage/eye irritation Category 1; Specific target organ toxicity Category 3; Hazard Statement. Molecular Weight 118.97 . A variant of the thionyl chloride battery, with 300 mV higher voltage. A sulfinyl halide in which both of the halide atoms are chorines. density 1.631 g/mL at 25 °C (lit.) Procedure excerpt: To a solution of the SM (2.63 g, 12.5 mmol) in DCM (60 mL) at 0 C was added DMF (0.49 mL, 6.3 mmol) followed by SOBr2 (1.26 mL, 16.3 mmol). A suspension of the SM (10 g, 78 mmol) in SOCl2 (35 mL) was refluxed for 4 h until the suspension became homogenous. Molar mass of SOCl2 = 118.9704 g/mol. 1-800-282-3982. SMILES string ClS(Cl)=O InChI ... General description Thionyl chloride is an inorganic acid chloride mainly used as a reagent to prepare carboxylic acid chlorides from carboxylic acids. New Jobs: ... Density: 2.683 g/mL. Packaging 5, 100 g in glass bottle Safety & Documentation. Density: 1.6400g/mL: Quantity: 25g: Safety and Handling . . Of 3-nitrobenzamide = 137.5 °C 2) NaOH OH 1) HNO3 OCH3 H2SO4 OCH3 3) HCl Experiment 7 & 8 NO2 NO2 Actual Yield % Yield X 100 Theoretical Yield Mass (g) Density = Volume (mL) Grams Mole = Molecular Weight Moles M= Moles = M X Liter Liter EXPERIMENTAL PROCEDURE 1. Thionyl chloride Product group Chlorination reagents Synonyms Sulfur oxychloride Sulfurous oxychloride IUPAC name Thionyl chloride Appearance Clear liquid, colourless to slightly yellow Applications Chlorinating agent for carboxylic acids, alcohols and active methylene compounds. Thionyl Chloride - chemical structure, common uses, and safety. Reagent for converting primary amides to nitriles. Passage of thionyl chloride through a flexible metal transfer hose which was contaminated with water or sodium hydroxide solution caused the hose to burst. [full procedure] References: 1) Patent … This product has been replaced by 230464|Sigma-Aldrich - Thionyl chloride, ReagentPlus, ≥99% | SOCl2 EC Number 231-748-8. Solubility (Other) Contents react with alcohols . . It has a role as a polar aprotic solvent and an EC 3.5.1.4 (amidase) inhibitor. Vapors are denser than air. [Note: Fumes form when exposed to moist air. H301, H311, H314, H331, H372, H400: GHS precautionary statements. Thionyl chloride solution 2.0 M in methylene chloride CAS Number 7719-09-7. Density, g.cm⁻³ : 1.64: Ionisation Energy, eV ... OSHA TWA PEL, mg.m⁻³: 5: View products detecting gaseous Thionyl chloride. C 3 H 7 NO. Product Details. Chemsrc provides Thionyl chloride(CAS#:7719-09-7) MSDS, density, melting point, boiling point, structure, formula, molecular weight etc. To a solution of the SM (1 g, 3.7 mmol) in MeOH (15 mL) was slowly added SOCl2 (5 mL) at 0 C. The reaction mixture was refluxed at 70 C for 2 h, after which time it was . Thionyl Chloride, Thionyl Chloride supplier, Thionyl Chloride distributor, CAS 7719-09-7, Thionyl Chloride manufacturer, Thionyl Chloride wholesale . Skip to main content. ], Skin: Prevent skin contact Eyes: Prevent eye contact Wash skin: When contaminated Remove: When wet or contaminated Change: No recommendation Provide: Eyewash, Quick drench, NIOSH REL : C 1 ppm (5 mg/m 3 ) OSHA PEL ? Science Supply Store offers Lab Supplies and Equipment, ECO Funnels, Nalgene Lab Bottles, Pharmacy Vials and Containers, Safety Storage Cabinets and Safety Cans SDS; CoA; Synonyms: Sulfurous acid dichloride, Sulfurous oxychloride Hill Formula: Cl₂OS EC Number: 231-748-8 Chemical Formula: SOCl₂ CAS #: 7719-09-7 Molar Mass: 118.97 g/mol. Reagent for converting carboxylic acids to acid chlorides. . It has been used in determination of atmospheric ammonia by denuder-sampling and HPLC-UV detection. Question: Weight Of 3-nitrobenzamide = 0.28 G M.p. : 7719-09-7 1.2 Relevant identified uses of the substance or mixture and uses advised against Identified uses : Laboratorychemicals, Industrial & for professional use only. Product name : Thionyl Chloride CAS-No. Interaction with water violently decomposes the chloride to hydrogen chloride (2 mol) and sulfur dioxide (1 mol), the total expansion ratio from liquid to gas being 993:1 at 20 deg C, so very high pressures may be generated. Safety and Handling. P260-P303+P361+P353-P305+P351+P338-P301+P330+P331-P405-P501a. Eye: Irrigate immediately Skin: Water flush immediately Breathing: Respiratory support Swallow: Medical attention immediately, inhalation, ingestion, skin and/or eye contact, Irritation eyes, skin, mucous membrane; eye, skin burns, Water, acids, alkalis, ammonia, chloryl perchlorate [Note: Reacts violently with water to form sulfur dioxide & hydrogen chloride. H314-Causes severe skin burns … density 1.173 g/mL at 25 °C (lit.) Read about company. 1 18.97 g/mol 1.64 g/cm ³-104 °C--1.5 mL; 2.46 g. M-T o luic A cid. The reaction mixture was then cooled . Application Thionyl chloride may be used in the following processes: PubChem Substance ID 24857637. Li-SO 2 Cl 2: Sulfuryl chloride: 3.7 V 3.95 V 330 720 Liquid cathode. SDS Certificate of Analysis (COA) Purchase; Safety & Documentation; Protocols & Articles; Peer-Reviewed Papers; Related Products; Purchase. . Thionyl Bromide - chemical structure, common uses, and safety. H302-Harmful if swallowed. Formula: Cl₂OS MW: 118.97 g/mol Boiling Pt: 76 °C (1013 hPa) Melting Pt: –104,5 °C Density: 1.64 g/cm³ (20 °C) Storage Temperature: Ambient: MDL Number: MFCD00011449 CAS Number: 7719-09-7 EINECS: 231-748-8 UN: 1836 ADR: 8,I Merck Index: 12,09485: Order Now. Linear Formula SOCl 2. . Density (g/ml) - 1.65 ± 0.05 (electrolyte); 0.53 ± 0.05 (lithium) Solubility (Water) Contents - Violently Reactive . Acetonitrile is a nitrile that is hydrogen cyanide in which the hydrogen has been replaced by a methyl group. Diethylamine. Specification Test Results. Safety Information. 808154 View Pricing & Availability. CopyCopied, Validated by Experts, Validated by Users, Non-Validated, Removed by Users, Predicted data is generated using the ACD/Labs Percepta Platform - PhysChem Module, Predicted data is generated using the US Environmental Protection Agency’s EPISuite™, Click to predict properties on the Chemicalize site, For medical information relating to Covid-19, please consult the, ACD/Labs Percepta Platform - PhysChem Module, US Environmental Protection Agency’s EPISuite™, Compounds with the same molecular formula, Search Google for structures with same skeleton, 168-170 F / 760 mmHg (75.5556-76.6667 °C / 760 mmHg), 169 F / 760 mmHg (76.1111 °C / 760 mmHg), Colorless to yellow to reddish liquid with a pungent odor like sulfur dioxide. Reagent for converting alcohols to chlorides. ], colourless, pale yellow or reddish liquid. It is a colorless, distillable liquid at room temperature and pressure that decomposes above 140 °C. Thionyl Chloride - Buy Thionyl Chloride at best price of Rs 500/500ml from Kishor Agencies. Lithium Thionyl Chloride Metal Batteries with Gallium Electrolyte Page: 2/6 Expiration Date: 24 May 2015 ... Vapor Density (Air=1) ~ 4 for electrolyte . Gascheck G helium leak detector. density of thionyl chloride is equal to 1 638 kg/m³; at 20°C (68°F or 293.15K) at standard atmospheric pressure.In Imperial or US customary measurement system, the density is equal to 102.3 pound per cubic foot [lb/ft³], or 0.9468 ounce per cubic inch [oz/inch³] . Cl 2 OS. Common Uses: Reagent for converting carboxylic acids to acid chlorides. The overall discharge reaction is as follows: Convert grams Thionyl Chloride to moles or moles Thionyl Chloride to grams. Reacts violently with water. The cells with added bromine chloride are thought to be safer when abused. Toxic by skin absorption. MDL number MFCD00011449. C 8 H 8 O 2. To a solution of the SM (294 g, 1.90 mol) in DCM (2.2 L) at -10 C was added SOCl2 (460 g, 3.90 mmol). Property Name Property Value Reference; Molecular Weight: 239.14 g/mol: Computed by PubChem 2.1 (PubChem release 2019.06.18) XLogP3: 4.1: Computed by XLogP3 3.0 (PubChem release 2019.06.18) PubChem Substance ID 329751670 Product Identifier. CopyCopied, InChI=1S/Cl2OS/c1-4(2)3 Related Categories: Alternative Energy, C … mol −1 Appearance Colorless to yellow liquid Density: 1.42 g/mL Melting point −22 °C (−8 °F; 251 K) Boiling point: 106 °C (223 °F; 379 K) Solubility in water . . ABOUT US; PRODUCTS; SUPPLIER PORTAL; QUALITY; NEWS; CAREERS; CONTACT; REGISTER / SIGN IN; Thionyl Chloride For more information call 1-800-282-3982 or email … Agent for O-sulfinylation and C-sulfinylation. Common Uses: Reagent for converting alcohols to bromides. The resulting mixture was refluxed for 2 h. The solvent was removed . 1-800-282-3982. Danger; Hazard Category. The mixture was allowed to . About Thionyl chloride; Thionyl chloride weighs 1.638 gram per cubic centimeter or 1 638 kilogram per cubic meter, i.e. The higher voltage drops back to 3.5 V soon as the bromine chloride gets consumed during the first 10–20% of discharge. CopyCopied, CSID:22797, http://www.chemspider.com/Chemical-Structure.22797.html (accessed 10:41, Dec 12, 2020) Also find here related product comparison | ID: 22108086048 Thionyl chloride; Signal Word. GasCheck G is a handheld gas leak detector for the rapid, effective detection of gas leaks providing reliable and stable readings of almost any gas or gas mixture. Thionyl dichloride weighs 1.638 gram per cubic centimeter or 1 638 kilogram per cubic meter, i.e. Thionyl chloride for synthesis, Sigma-Aldrich® Thionyl chloride. NACRES NA.21 . Thionyl chloride ≥98% CAS Number 7719-09-7. Flash point 42°F. C 4 H 10 O. SMILES string Cc1cccc(c1)C(Cl)=O InChI 1S ... m-Toluoyl chloride has been used to derivatize the C 1-C 4 aliphatic amines for their determination in air by HPLC. Antares Chem Private Limited - Offering Thionyl Chloride, Density: 1.64 G/Cm3 at Rs 150/kilogram in Mumbai, Maharashtra. O=S(Cl)Cl . C 4 H 1 1 N. 73.137 g/mol 0.707 g/mL-50 °C 5 mL; 3.535 g. Diethyl Ether. Incompatible with most commonmetals, strong reducing agents, strong bases, alcohols, amines. Density (g/ml) MPLit (°C) MP Observ ed (°C) Quantity (g) Thionyl Chloride. The resulting mixture was refluxed for 2 h. The solvent was removed . A mixture of the SM (1.0 g, 6.3 mmol) in ACN (20 mL) was treated with SOCl2 (0.8 mL). Beilstein/REAXYS Number 1209273 . MDL number MFCD00011449. . Partition Coefficient (n-Octanol/water) - Reactive . Density 0.783 g / cm3. Thionyl chloride is a component of lithium–thionyl chloride batteries, where it acts as the positive electrode (cathode) with lithium forming the negative electrode (anode); the electrolyte is typically lithium tetrachloroaluminate. Molecular Weight 118.97 . Get contact details and address | ID: 11667347988 density of thionyl chloride. The reaction mixture was stirred at reflux for 1 h. The mixture was . All density of thionyl chloride wholesalers & density of thionyl chloride manufacturers come from members. . Properties. Less dense than water. New Jobs: ... Density: 1.631 g/mL. 20 g/mL Merck Millipore 1117: 20 g/l Merck Millipore 808154: 1.35 g/mL Alfa Aesar H31857: 1.631 g/l SynQuest M016-4-01: 1.64 g/l Parchem – fine & specialty chemicals 89100: 1.64 g/l Wikidata Q409171: 1.631 g/mL Sigma-Aldrich SIAL-18438: 1.679 g/mL / 20 °C Kaye & Laby (No longer updated) . CopyCopied, FYSNRJHAOHDILO-UHFFFAOYSA-N Reagent for converting carboxylic acids to esters. Articles of Thionyl chloride are included as well. Molecular weight calculation: 32.065 + 15.9994 + 35.453*2 ›› Percent composition by element. Similar to thionyl chloride. Thionyl chloride MSDS (material safety data sheet) or SDS, CoA and CoQ, dossiers, brochures and other available documents. Synthesis of heterocyclic compounds Other properties: Odour: … : none. Density: 2.688 g/mL, liquid Melting point −52 °C (−62 °F; 221 K) Boiling point : 68 °C (154 °F; 341 K) at 40 mmHg Solubility in water. Safety glasses, gloves, good ventilation. . Linear Formula SOCl 2. 73.09 g/mol---61 °C--1 drop. Density of Thionyl chloride g cm3 = 1.638 g/cm³ Density of Thionyl chloride g ml = 1.638 g/ml Density of Thionyl chloride g mm3 = 0.001638 g/mm³ Density of Thionyl chloride kg m3 = … 1) Patent Reference: WO2010016005, page 89, (11.3 MB), 2) Patent Reference: WO2010038081, page 128, (33.8 MB), 3) Patent Reference: WO2016014463, page 91, (6.7 MB), 4) Patent Reference: WO2010104899, page 155, (6.7 MB), 6) www.sigmaaldrich.com: Thionyl chloride (link). density of thionyl dichloride is equal to 1 638 kg/m³; at 20°C (68°F or 293.15K) at standard atmospheric pressure.In Imperial or US customary measurement system, the density is equal to 102.3 pound per cubic foot [lb/ft³], or 0.9468 ounce per cubic inch [oz/inch³] . Reacts Vapor pressure: 19 mmHg (20°C) Hazards Safety data sheet: Oxford MSDS: GHS pictograms: GHS Signal word: Danger: GHS hazard statements. Quantity: 25g: safety and Handling lit. chloride wholesale: weight of 3-nitrobenzamide = 0.28 g M.p g/mL-50... 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